The distribution of Fe3+ and Ni2+ over the four crystallographically distinct octahedral cation sites in FeNi2BO5 has been precisely determined from a single resonant powder X-ray pattern collected 16 eV below the Fe K absorption edge and is very similar to that in AlNi2BO5, showing that charge rather than size determines the cation distribution in these borates.
D. A. Perkins and J. P. Attfield, J. Chem. Soc., Chem. Commun., 1991, 229 DOI: 10.1039/C39910000229
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