The synthesis of [3,4-3H]but-3-enylglucosinolate is described and its role in (R)-2-hydroxybut-3-enylglucosinolate biosynthesis is discussed. This is the first time radio labelled but-3-enylglucosinolate has been synthesized and its incorporation into (R)-2-hydroxybut-3-enylglucosinolate demonstrated.
J. T. Rossiter and D. C. James, J. Chem. Soc., Perkin Trans. 1, 1990, 1909 DOI: 10.1039/P19900001909
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