The (±)-trimethyl ether of the unusual heterocycle peltogynol (3; R = OMe), and its ring skeleton (9; R = H), have been synthesised via 6-endo intracyclisation of the radical derived from the iodides (8; R = H) and (8; R = OMe).
S. A. Ahmad-Junan and D. A. Whiting, J. Chem. Soc., Perkin Trans. 1, 1990, 418 DOI: 10.1039/P19900000418
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