The redox process of methylene blue has been studied using thin-layer cyclic voltammetry, UV–VIS spectroelectrochemical techniques and in situ EPR. In situ EPR measurements provide direct evidence for the formation of a methylene blue cation radical. The electrode mechanism for methylene blue is discussed.
R. Zhan, S. Song, Y. Liu and S. Dong, J. Chem. Soc., Faraday Trans., 1990, 86, 3125 DOI: 10.1039/FT9908603125
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