A gas-phase electron diffraction study of dimethyl(2,4-pentanedionato)gold(III) indicates a square-planar structure with ra(Au–O)= 2.085(7), ra(Au–C)= 2.054(5)Å, angle OAuO 90.9(6)°, and CAuC 92.7(24)°, as well as the normal parameters of an acetylacetone ligand.
S. Shibata, K. Iijima and T. H. Baum, J. Chem. Soc., Dalton Trans., 1990, 1519 DOI: 10.1039/DT9900001519
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