The reaction of 2, 4, 6-trimethoxyphenyl-lead triacetate (4) with 3,5-di-t-butylphenol (1) at room temperature afforded the very hindered phenol (5) in good (87%) yield; acetylation gave the acetate (7) which was fully characterised, including an X-ray determination.
D. H. R. Barton, D. M. X. Donnelly, P. J. Guiry and J. H. Reibenspies, J. Chem. Soc., Chem. Commun., 1990, 1110 DOI: 10.1039/C39900001110
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