A mononuclear superoxo cobalt(III) complex generated by the oxgenation of a CoII–([14]aneN4) complex ([14]aneN4= 1,4,8,11-tetra-azacyclotetradecane) in an aqueous solution containing a large excess of dioxygen was found to be able to exist in equilibrium with the [{Co([14]aneN44)(OH2)}2O2]4+ ion, which was stable at room temperature.
N. Shinohara, K. Ishii and M. Hirose, J. Chem. Soc., Chem. Commun., 1990, 700 DOI: 10.1039/C39900000700
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