The synthesis of 12-bromo- and 12-chloro-forskolin was accomplished by TBAF promoted halogenation of suitably protected silyl enol ethers, while reaction of a lithium enolate with acetyl hypofluorite gave 12-fluoroforskolin.
G. M. Shutske, J. Chem. Soc., Perkin Trans. 1, 1989, 1544 DOI: 10.1039/P19890001544
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