Intramolecular 1,5-transfer of a primary hydrogen atom is the dominant behaviour in dioxyl diradicals formed by flash vacuum pyrolysis of 5-substituted 3-methyl-1,2-dioxanes and is followed by decarbonylation when the substituent is the vinyl group.
A. J. Bloodworth and R. J. Curtis, J. Chem. Soc., Chem. Commun., 1989, 1674 DOI: 10.1039/C39890001674
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