The Sn–Cl distances in octahedral SnCl4L2 compounds are linearly related to the Mössbauer partial quadrupole splitting data; the correlation can be used to predict Sn–Cl distances, and has allowed us to detect an error in the published crystal structure of tetrachlorobis(1,3-diethylthiourea)tin(IV) which was confirmed in a redetermination.
D. Tudela, M. A. Khan and J. J. Zuckerman, J. Chem. Soc., Chem. Commun., 1989, 558 DOI: 10.1039/C39890000558
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