Base hydrolysis of (η5-C5Me5)ZrCl3 in tetrahydrofuran (THF) yields [(η5-C5Me5)ZrCl]3(O)(OH)4·2THF which, according to X-ray structural analysis, contains a triangular Zr3 core capped above and below by µ3-O and µ3-OH groups and edge-bridged by three µ2-OH groups.
L. M. Babcock, V. W. Day and W. G. Klemperer, J. Chem. Soc., Chem. Commun., 1988, 519 DOI: 10.1039/C39880000519
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