An X-ray crystallographic analysis of ReO2(CH2CMe3)3 and variable temperature 1H n.m.r. studies involving ReO2R3, R = CH2CMe3 or CH2SiMe3, suggest that α-C–H ⋯ O![[double bond, length as m-dash]](https://www.rsc.org/images/entities/char_e001.gif)
Re interactions occur in the complexes.
S. Cai, D. M. Hoffman and D. A. Wierda, J. Chem. Soc., Chem. Commun., 1988, 313 DOI: 10.1039/C39880000313
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