The reaction of ClAuPPh3 with sodium 3,5-diphenylpyrazolate in tetrahydrofuran with added AgOCOPh yields hexakis(µ-3,5-diphenylpyrazolato-N,N′)-hexagold(I)(1), a compound with a novel 18-membered twisted ring and a fused-edge bi-tetrahedral grouping of gold atoms, as determined crystallographically.
R. G. Raptis, H. H. Murray and J. P. Fackler, J. Chem. Soc., Chem. Commun., 1987, 737 DOI: 10.1039/C39870000737
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