(±)-myo-Inositol 4,5-bisphosphate was synthesized using a phosphite chemistry approach; bisphosphorylation was confirmed by the observation of the first 5JPP coupling in a bisphosphite triester intermediate.
M. R. Hamblin, B. V. L. Potter and R. Gigg, J. Chem. Soc., Chem. Commun., 1987, 626 DOI: 10.1039/C39870000626
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