The synthesis of tris(pentachlorophenyl)silane (1), perchlorotriphenylsilane (2), and bromotris(pentachlorophenyl)silane (3) are reported for the first time, the hydrolysis of (2) and (3) under neutral conditions giving tris(pentachlorophenyl)silanol (4); the structure of the silane (2) has been established by X-ray crystallography.
L. Fajarí, L. Juliá, J. Riera, C. Miravitlles and E. Molins, J. Chem. Soc., Chem. Commun., 1987, 143 DOI: 10.1039/C39870000143
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