Gas chromatographic method for the determination of isomeric bromoisobutyric acids and their chlorides
Abstract
A GC method for the determination of 3-bromoisobutyric acid and the isomeric 2-bromoisobutyric acid, 2,3-dibromoisobutyric acid and methacrylic acid as their trimethylsilyl esters was developed. The determination of the corresponding acid chlorides was performed after their conversion to the corresponding morpholides.