One-bond C–H coupling constants of the anionic carbon of anions derived from disulphones (1)–(3) provide unequivocal evidence for the trigonal hybridization of the charged carbon, previously assigned as tetrahedral; it is shown that the 1,3-dithiolane 1,1,3,3-tetraoxide undergoes ring opening upon treatment with strong bases.
A. Berlin, S. Bradamante, R. Ferraccioli and G. A. Pagani, J. Chem. Soc., Chem. Commun., 1986, 1191 DOI: 10.1039/C39860001191
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