The single crystal X-ray structure of the title complex (1) shows that two MoO(O2)2 moieties are spanned by a tartrato ligand which is bidentate at each end, giving pentagonal bipyramidal co-ordination to the molybdenum atoms; spectroscopic data (13C, 95Mo n.m.r., Raman) show that this structure is maintained in aqueous solution.
A. C. Dengel, W. P. Griffith, R. D. Powell and A. C. Skapski, J. Chem. Soc., Chem. Commun., 1986, 555 DOI: 10.1039/C39860000555
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