The new chiral macrocyclic polyhydroxy ethers (5) and (8) were prepared by treatment of β- and α-cyclodextrins with diethylborane and 9-borabicycle[3.3.1]nonan-9-yl methanesulphonate as catalyst.
M. Bernabé, M. Martin-Lomas, S. Penadés, R. Köster and W. V. Dahlhoff, J. Chem. Soc., Chem. Commun., 1985, 1001 DOI: 10.1039/C39850001001
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