29 Si magic angle spinning n.m.r experiments on highly siliceous ZSM-5 have shown that there is a phase transition in the temperature range 295–363 K in agreement with the results of powder X-ray diffraction measurements.
C. A. Fyfe, G. J. Kennedy, G. T. Kokotailo, J. R. Lyerla and W. W. Fleming, J. Chem. Soc., Chem. Commun., 1985, 740 DOI: 10.1039/C39850000740
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