Thermolysis of the dispiro-trioxane (2) in decane at 190 °C afforded a novel nine-membered ring lactone whose structure has been determined by X-ray crystallography.
B. Kerr and K. J. McCullough, J. Chem. Soc., Chem. Commun., 1985, 590 DOI: 10.1039/C39850000590
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