1,3λ4δ2,5,2,4-Trithiadiazepine (6) and its benzo derivative (4) are stable crystalline compounds which are synthesised from bis(sulphenyl chlorides) and bis(trimethylsilyl)sulphurdiimide; spectroscopic and chemical properties show the heterocyclic ring to be a 10π aromatic system.
J. L. Morris, C. W. Rees and D. J. Rigg, J. Chem. Soc., Chem. Commun., 1985, 396 DOI: 10.1039/C39850000396
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