Electrochemical doping and undoping by cations such as tetraethylammonium was first performed with a polythienylene thin film, which was synthesized by the electrochemical oxidative polymerization of thiophene in an acetonitrile solution in the potential range below –1.5 V vs. Ag/AgCl.
M. Aizawa, S. Watanable, H. Shinohara and H. Shirakawa, J. Chem. Soc., Chem. Commun., 1985, 264 DOI: 10.1039/C39850000264
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