The reaction of [Mo2(CO)4(µ,η2-MeCO)(η-C5H5)2][BF4] with LiEt3BH and of [Mo(CO)2(η2-MeCHO)(η-C5H5)]– with [C7H7][BF4] or [Mo(CO)3(C7H7)][BF4] or [Mo(CO)3(η-C5H5)][BF4] or CH2Cl2 have as common product the bridging acetaldehyde complex Mo2(CO)4(µ,η2-MeCHO)(η-C5H5)2 which is the subject of an X-ray crystallographic study.
H. Adams, N. A. Bailey, J. T. Gauntiett and M. J. Winter, J. Chem. Soc., Chem. Commun., 1984, 1360 DOI: 10.1039/C39840001360
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