N.m.r. spectra of highly reduced vanadium carbonyls containing 99% enriched 13CO in liquid ammonia at –50 °C provide the first direct spectroscopic evidence for the existence of Na3[V(CO)5] and Na2[HV(CO)5] in solution.
G. F. P. Warnock, S. B. Philson and J. E. Ellis, J. Chem. Soc., Chem. Commun., 1984, 893 DOI: 10.1039/C39840000893
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