A 3 : 1 mixture of H2 : CO (total pressure 1 atm) is converted with ca. 20% efficiency and ca. 95% selectivity into acetylene at 100°C over a catalyst generated by partially de-intercalating a (first stage) sandwich compound C9FeCl3 with potassium naphthalenide: the catalyst maintains its performance for several days under these conditions.
W. Jones, R. Schlögl and J. M. Thomas, J. Chem. Soc., Chem. Commun., 1984, 464 DOI: 10.1039/C39840000464
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