The composition of the (Na, TPA)(TPA = tetrapropylammonium) precursor to silicalite-1 is determined by the base content of the reaction mixture, and for both low and high base contents the crystallization is accompanied by apparently anomalous pH changes.
S. G. Fegan and B. M. Lowe, J. Chem. Soc., Chem. Commun., 1984, 437 DOI: 10.1039/C39840000437
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