1H-Cyclobuta[de]naphthalene is preparable by reactions of 1,8-dilithionaphthalene with dichloromethane and 1,8-bis(iodomagnesio)naphthalene with methylene bis(toluene-p-sulphonate).
L. S. Yang, T. A. Englear and H. Shechter, J. Chem. Soc., Chem. Commun., 1983, 866 DOI: 10.1039/C39830000866
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