A convenient method for the synthesis, by the phosphotriester approach, of dinucleoside phosphorothioates is illustrated by the preparation and isolation of the pure Rp- and Sp-diastereoisomers of thymidine-3′ thymidine-5′ phosphorothioate (5).
Ö. Kemal, C. B. Reese and H. T. Serafinowska, J. Chem. Soc., Chem. Commun., 1983, 591 DOI: 10.1039/C39830000591
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