The first syntheses of Laurencia-derived cyclic ethers containing terminal cis-enyne side chains are reported which employ (for the first time in complex natural product synthesis) a recently developed partial catalytic hydrogenation of a silylated butadiyne derivative which, in turn, is derived from bis(trimethylsilyl)butadiyne.
A. B. Holmes, C. L. D. Jennings-White and D. A. Kendrick, J. Chem. Soc., Chem. Commun., 1983, 415 DOI: 10.1039/C39830000415
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