1 H N.m.r. spectroscopy can readily distinguish endo- and exo-6-substituted bicyclo[3.1.0]hex-2-enes. Nuclear Overhauser measurements coupled with resolution enhancement techniques and T1 values have permitted a full assignment of the 1H n.m.r. parameters.
P. Barraclough, D. W. Young, A. G. Ferrige and J. C. Lindon, J. Chem. Soc., Perkin Trans. 2, 1982, 651 DOI: 10.1039/P29820000651
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