Routes to the preparation of αβ-unsaturated ketones (1k–m) have been investigated. n-Butylmanganese(II) chloride was particularly useful for preparing the ketones (1m) from the readily available monic acid A (1b), the nucleus of pseudomonic acid A (1a).
S. Coulton, P. J. O'Hanlon and N. H. Rogers, J. Chem. Soc., Perkin Trans. 1, 1982, 729 DOI: 10.1039/P19820000729
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