A radical cation generated electrochemically in acetonitrile at 243 K from N-nitroso-2,2,6,6-tetramethylpiperidine gave an e.s.r. spectrum with the largest known nitrogen hyperfine splitting constant for an organic compound (45.0 G) and with long range couplings to hydrogen atoms.
M. Masui, K. Nose, H. Ohmori and H. Sayo, J. Chem. Soc., Chem. Commun., 1982, 879 DOI: 10.1039/C39820000879
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