Mo6O10(OPri)12, an intermediate in the reaction between Mo2(OPri)6 and molecular oxygen which yields [MoO2(OPri)2]n, has been structurally characterized and found to contain a serpentine chain of molybdenum atoms connected by bridging oxo-and alkoxy-ligands; there is also a pair of alkoxy-ligands which are semibridging.
M. H. Chisholm, K. Folting, J. C. Huffman and C. C. Kirkpatrick, J. Chem. Soc., Chem. Commun., 1982, 189 DOI: 10.1039/C39820000189
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