Both the anion and dianion of CO2 have been detacted by i.r matrix isolation spectroscopy as reactive intermediates in the reductive coupling of CO2 by lithium atom to give lithium oxalate.
R. H. Hauge, J. L. Margrave, J. W. Kauffman, N. A. Rao, M. M. Konarski, J. P. Bell and W. E. Billups, J. Chem. Soc., Chem. Commun., 1981, 1258 DOI: 10.1039/C39810001258
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