The new, neutral mixed-metal cluster (η-C5H5)3Ni3Os3(CO)9 has been obtained in good yield from a simple pyrolytic reaction; the metal-atom arrangement has been shown by X-ray crystallography to be a face-capped trigonal bipyramid.
E. Sappa, M. Lanfranchi, A. Tiripicchio and M. T. Camellini, J. Chem. Soc., Chem. Commun., 1981, 995 DOI: 10.1039/C39810000995
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