2,2,2-Trichloroethoxycarbonylphosphonates were converted directly by treatment with Zn–Me3SiCl into silyl phosphites which in situ reacted with aldehydes to give α-hydroxyphosphonates in good yields.
M. Sekine, H. Yamagata and T. Hata, J. Chem. Soc., Chem. Commun., 1981, 970 DOI: 10.1039/C39810000970
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