An X-ray crystal structure determination shows the gold(I) complex with four methyldiphenylphosphine ligands to have ![[4 with combining macron]](https://www.rsc.org/images/entities/char_0034_0304.gif)
symmetry with all Au–P bond lengths equal and nearly tetrahedral angles; further, 31P n.m.r. spectroscopy at –80 °C indicates that the nearly tetrahedral species persists in solution.
R. C. Elder, E. H. K. Zeiher, M. Onady and R. R. Whittle, J. Chem. Soc., Chem. Commun., 1981, 900 DOI: 10.1039/C39810000900
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