Mixed-valence iodide-bridged compounds of rhenium have been obtained by the di-iodine oxidation of rhenium(I) carbonyl complexes; the X-ray crystal and molecular structure of Re3I6(CO)6, a ReI–ReIV complex of S6 symmetry, is presented.
F. Calderazzo, F. Marchetti, R. Poli, D. Vitali and P. F. Zanazzi, J. Chem. Soc., Chem. Commun., 1981, 893 DOI: 10.1039/C39810000893
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