Thermal rearrangement of the endo-peroxides of the 2,5-dimethylfurans (1b) and (1c) in refluxing benzene leads to the corresponding diepoxides (4b) and (4c), which provides a convenient entry to the synthesis of these compounds which are structurally related to crotepoxide.
M. L. Graziano, M. R. Iesce and R. Scarpati, J. Chem. Soc., Chem. Commun., 1981, 720 DOI: 10.1039/C39810000720
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