Trapping of phenyl radicals produced by thermal decomposition of phenylazo p-tolyl sulphone (4a) by toluene-p-sulphonyl iodide is an effective way to generate toluene-p-sulphonyl radicals uncomplicated by the presence of phenyl radicals.
C. M. M. da Silva Corrêa, J. Chem. Soc., Perkin Trans. 1, 1979, 1519 DOI: 10.1039/P19790001519
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