Issue 20, 1979
From the journal:

Journal of the Chemical Society, Chemical Communications

Preparation and X-ray crystal structure of µ-iodo-bis(4-iodo-cyclo-hepta-sulphur) tris(hexafluoroantimonate)–bis(arsenic trifluoride), [(S7I)2I]3+[SbF6]–3·2AsF3

Jack Passmore,   George Sutherland  and  Peter S. White  

Abstract

The reaction of S8, I2, and SbF5 in the appropriate ratios in AsF3 gave essentially quantitative yields of S14I3(SbF6)3·2AsF3, shown by X-ray crystallography to contain the novel cation [(S7I)2I]3+, consisting of two [S7I]+ fragments bridged by a linear S–I–S bond.

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Article information

DOI
https://doi.org/10.1039/C39790000901
Article type
Paper

J. Chem. Soc., Chem. Commun., 1979, 901-902

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Preparation and X-ray crystal structure of µ-iodo-bis(4-iodo-cyclo-hepta-sulphur) tris(hexafluoroantimonate)–bis(arsenic trifluoride), [(S7I)2I]3+[SbF6]–3·2AsF3

J. Passmore, G. Sutherland and P. S. White, J. Chem. Soc., Chem. Commun., 1979, 901 DOI: 10.1039/C39790000901

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