Most base–solvent combinations convert (2) into (3); γ-alkylation to yield (5) is effected by sodium hydroxide in dimethyl sulphoxide–water mixtures in which the water content is critical.
A. P. Johnson and V. Vajs, J. Chem. Soc., Chem. Commun., 1979, 817 DOI: 10.1039/C39790000817
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