X-Ray studies show that the blue crystalline isopropylammonium salt, isolated following the photoreduction of (NH3Pri)6(Mo7O24) in aqueous solution, contains Mo13O404–(mixed-valence) and H4Mo12O404–, both having the Keggin structure, randomly distributed over the anion sites in a 1 : 2 ratio.
T. Yamase, T. Ikawa, Y. Ohashi and Y. Sasada, J. Chem. Soc., Chem. Commun., 1979, 697 DOI: 10.1039/C39790000697
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