1  H n.m.r. determination of enantiomeric purities of 2-substituted aldehydes via the aldimine of 2-amino-1-methoxymenth-8-ene

A. I. Meyers; Zdenek Brich

doi:10.1039/C39790000567

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¹H n.m.r. determination of enantiomeric purities of 2-substituted aldehydes via the aldimine of 2-amino-1-methoxymenth-8-ene

A. I. Meyers and Zdenek Brich

Abstract

The aldimine proton (R–CH [double bond, length half m-dash] NR) from aldehydes and the titled compound exhibits diastereomeric non-equivalence in the ¹H n.m.r. spectrum allowing determination of the enantiomeric excess for 2-substituted aldehydes.

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DOI: https://doi.org/10.1039/C39790000567
Article type: Paper

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J. Chem. Soc., Chem. Commun., 1979, 567-568

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¹ H n.m.r. determination of enantiomeric purities of 2-substituted aldehydes via the aldimine of 2-amino-1-methoxymenth-8-ene

A. I. Meyers and Z. Brich, J. Chem. Soc., Chem. Commun., 1979, 567 DOI: 10.1039/C39790000567

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Journal of the Chemical Society, Chemical Communications