Methyl 3-hydroxycyclohexa-1,5-diene-1-carboxylate (10) is prepared in two steps from methyl cyclohexa-2,5-diene-1-carboxylate (7), and its dehydration, hydrolysis, acetylation, reduction, and epoxidation are reported, together with its Diels–Alder reaction with 4-phenyl-1,2,4-triazoline-3,5-dione.
H. M. Sirat, E. J. Thomas and N. D. Tyrrell, J. Chem. Soc., Chem. Commun., 1979, 36 DOI: 10.1039/C39790000036
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