Conjugated addition of Grignard reagents to nitro-compounds provides a new method of synthesis for alkyl-nitrosoderivatives in the naphthalene, quinoline, indole, benzothiophen, benzoxazole, and benzothiazole series. The mechanism is discussed. Detailed mass spectra as well as 1H n.m.r. spectra are reported for unknown nitroso-compounds.
G. Bartoli, R. Leardini, A. Medici and G. Rosini, J. Chem. Soc., Perkin Trans. 1, 1978, 692 DOI: 10.1039/P19780000692
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