The anodic oxidation of 1H-perfluoroalkanes in HSO3F–KSO3F (0·5M) leads to perfluoroalkyl fluorosulphates, through an indirect process as confirmed by 19F C.I.D.N.P.
A. Germain and A. Commeyras, J. Chem. Soc., Chem. Commun., 1978, 118b DOI: 10.1039/C3978000118B
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