Anodic functionalization of 1H-perfluoroalkanes. Observation of 19F C.I.D.N.P.
Abstract
The anodic oxidation of 1H-perfluoroalkanes in HSO3F–KSO3F (0·5M) leads to perfluoroalkyl fluorosulphates, through an indirect process as confirmed by 19F C.I.D.N.P.