1 H and 31P N.m.r. studies of scandium(III)–trimethyl phosphate (TMP) solutions show that [Sc(TMP)6]3+[J(45Sc–31P)ca. 35 Hz] is the greatly predominant scandium(III) species in solution, and that its lability towards ligand exchange is intermediate between that of the analogous aluminium(III) and magnesium(II) species.
D. L. Pisaniello, S. F. Lincoln and E. H. Williams, J. Chem. Soc., Chem. Commun., 1978, 1047 DOI: 10.1039/C39780001047
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