Oxidation of N-phenyl-N′-trimethylsilylhydrazine (1) with dimethyl azodicarboxylate gives high yields of phenyltrimethylsilyldiazene (2), which reacts with sodium methoxide in tetrahydrofuran to give the synthetic equivalent of the phenyl anion.
J. C. Bottaro, J. Chem. Soc., Chem. Commun., 1978, 990 DOI: 10.1039/C39780000990
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